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华南理工大学大学化学与化工学院导师：祝诗发正文
姓名：祝诗发 性别：男 职称：副教授
学院：化学与化工学院 最后学历：博士
主要研究方向：有机合成、药物合成、金属有机、不对称有机合成
祝诗发，博士，副教授，硕士生导师。2001年6月本科毕业于湖南大学化学化工学院，同年考入中科院上海有机所硕博连读，导师朱仕正研究员，2006年6月获中科院上海有机所理学博士学位。同年9月赴美，先后在Syracuse University和University of South Florida从事博士后研究，主要研究方向为金属催化不对称有机合成。2009年5月，作为“海外优秀引进人才”进入华南理工大学化学与化工学院工作，2011年入选“教育部新世纪优秀人才支持计划”。已在J. Am. Chem. Soc., Angew. Chem. Int. Ed., Org. Lett., JOC等杂志上发表SCI 论文近30篇，申请中国专利7项，美国专利2项，目前主要从事过渡金属催化有机合成方面的研究工作。
主要学习工作经历：
1997.09－2001.07 湖南大学化学化工学院，获学士学位
2001.09－2006.07 中国科学院上海有机所，获博士学位
2006.09－2007.01 Syracuse University化学系，博士后研究
2007.01－2008.12 University of South Florida化学系，博士后研究
2009.03－今 华南理工大学化学与化工学院海外优秀人才引进计划, 副教授
研究兴趣：
有机合成；药物合成；金属有机化学；不对称有机合成；目前已发表文章近30篇，申请美国专利2篇、中国专利7篇
近年来主持的部分科研项目：
1. 教育部新世纪优秀人才支持计划，（主持），2011.1-2013.12
2. 国家自然科学基金面上项目（主持），2012.1-2015.12；
3. 国家自然科学基金青年科学基金项目（主持），2010.1-2012.12
4. 广东省自然科学基金博士启动基金（主持），2009.10-2011.9；
5. 华南理工大学中央高校基本科研业务费（主持），2010.1-2012.12
6. 华南理工大学科研启动费（主持），2010.1-2012.12
7. 中科院上海有机所氟化学重点实验室开放基金 (主持), 2010.11-2012.10
8. 温州大学有机化学与皮革化工重中之重学科开放基金 (主持), 2010.11-2012.10
9 广东省自然科学基金团队项目（参与），2011.1-2013.12
10.国家科技支撑973项目（参与），2011.01-2015.08
代表文章
1. Shifa Zhu*, Chao Wang, Lijuan Chen, Renxiao Liang, Yinfeng Yu, Huanfeng Jiang. Modular Approach for Synthesis of Vicinal Diamines Containing Axial Chiral 1,1′-Binaphthyl from 1,2-Diaminoethane by Pd-Catalyzed N-Arylation Reactions, Org. Lett. 2011, 13, 1146-1149.
2.
3. Shifa Zhu*, Lijuan Chen, Renxiao Liang, Chao Wang, Xiujun Wang, Yanwei Ren, Huanfeng Jiang. A practical system to synthesize the multiple-substituted 2,5-dihydrofuran by the intermolecular dipolar cycloaddition reactions involving acceptor/acceptor substituted diazo reagents. Tetrahedron 2011, 67, 5507-5515.
4. Shifa Zhu, Xue Xu, Jason Perman, Peter X. Zhang*. A General and Efficient Cobalt(II)-Based Catalytic System for Highly Stereoselective Cyclopropanation of Alkenes with alfa-Cyanodiazoacetates J. Am. Chem. Soc., 2010, 132, 12796-12799.
5. Shifa Zhu, Joshua V. Ruppel, Hongjian Lu, Lukasz Wojtas, Peter X. Zhang*. Cobalt-Catalyzed Asymmetric Cyclopropanation with Diazosulfones: Rigidification and Polarization of Ligand Chiral Environment via Hydrogen Bonding and Cyclization. J. Am. Chem. Soc., 2008, 130, 5042-5043. (Highlighted by SYNFACTS, 2008, 7, 720. and Angew. Chem. Int. Ed., 2009, 48, 850.)
6. Shifa Zhu, Jason Perman, X. Peter Zhang*. Acceptor/Acceptor-Substituted Diazo Reagents for Carbene Transfers: Cobalt-Catalyzed Asymmetric Z-Cyclopropanation of Alkenes with α-Nitro-Diazoacetates. Angew. Chem., Int. Ed., 2008, 47, 8460-8463. (Highlighted by SYNFACTS, 2009, 1, 74. and Angew. Chem. Int. Ed., 2009, 48, 850.)
7. Xin Cui, Xue Xu, Hongjian Lu, Shifa Zhu, Lukasz Wojtas, and X. Peter Zhang*, Enantioselective Cyclopropenation of Alkynes with Acceptor/Acceptor-Substituted Diazo Reagents via Co(II)-Based Metalloradical Catalysis. J. Am. Chem. Soc., 2011, 133, 3304-3307.
8. Shifa Zhu, Yuanxi Liao, Shizheng Zhu*. Transition-Metal-Catalyzed Formation of trans Alkenes via Coupling of aldehydes. Org. Lett. 2004, 6, 377-380.
9. Velusamy Subbarayan, Joshua V.Ruppel, Shifa Zhu, Jason A. Perman, X. Peter*. Zhang, Highly Asymmetric Cobalt-Catalyzed Aziridination of Alkenes with Trichloroethoxysulfonyl Azide (TcesN3). Chem. Commun. 2009, 28, 4266-4268.
10. Shifa Zhu, Yuanxi Liao, Shizheng Zhu*. The First Example of Catalytic Aziridination Mediated by Arsonium Ylides: Preparation of trans Pentafluorophenyl-Containing Aziridines, Synlett 2005, 1429-1432.
11. Shizheng Zhu*, Shifa Zhu, Guifang Jin, and Zhanting Li*. Strong Phenyl- perfluorophenyl - Stacking Interactions and C-H…F-C Hydrogen Bonding Interactions in The Crystalline of Corresponding Aromatic aldimines. Tetrahedron Letters 2005, 46, 2713-2716.
12. Shifa Zhu, Chunhui Xing, Shizheng Zhu*. Stereoselective Preparation of Trifluoromethyl Containing 1,4-Oxathiolane Derivatives Through Ring Expansion Reaction of 1,3-Oxathiolanes, Tetrahedron 2006, 62, 829–832.
13. Shizheng Zhu*, Shifa Zhu, Yuanxi Liao. Rhodium(II)-Catalyzed Addition of 2-Diazo(fluoroalkyl)acetoacetates to Sulfides: a Simple Synthesis of Stable Sulfonium Ylides. Journal of Fluorine Chemistry 2004, 125, 1071–1076.
14. Shifa Zhu, Shizheng Zhu*, Yuanxi Liao, Chaofeng Huang, Zhanting Li*. Co-existing Intermolecular Halogen Bonding and Hydrogen Bonding in the Compound Trans-5,10-bis(1-bromodifluoroacetyl-1-ethoxycarbonyl-methylidene) Thianthrene. Chinese Journal of Chemistry 2004, 22, 896-898.
15. Shifa Zhu, Shizheng Zhu*. Rh2(OAc)4-Catalyzed Formation of trans Alkenes From the Reaction of Aldehydes with Perfluorophenyl Diazomethane Through Tellurium Ylide. Tetrahedron Lett. 2006, 47, 5897-5900.
16. Shifa Zhu, Wan Pang, Chunhui Xing, Shizheng Zhu, Lewis Base-Catalyzed Formation of α-Trifluoromethyl Alcohol from CF3SiMe3 and Carbonyl-Containing Compounds, Chinese Journal of Chemistry, 2007, 25, 2, 233-236.
17. Ruixin Zhu, Shifa Zhu, Junhong Zhou, Minbo Chen*. The Atoms in Molecules (AIM) Analysis of Abnormal Bonding of Several Fluorinated Supramolecular Systems, Acta Chimica Sinica 2006, 164, 191-197.
18. Wan Pang, Shifa Zhu, Huanfeng jiang and Shizheng Zhu*. Transition metal-catalyzed formation of CF3-substituted α,β-unsaturated alkene and the synthesis of α-trifluoromethyl substituted β-amino ester. Tetrahedron 2006, 62, 11760-11765.
19. Chunhui Xing, Xianfu Li, Shifa Zhu, Shizheng Zhu*. Synthesis of (E)-α-Per(poly)fluoroalkanesulfonyl- α,β-unsaturated Ketones and their Hetero Diels-Alder Reactions with Vinyl Ether, Tetrahedron Lett. 2006, 47, 4951-4955.
20. Hui wang, Shifa Zhu, Qinying Deng*, ShiZheng Zhu*. A facile synthesis of 4-gem-difluoromethylene β-lactam and its derivatives from BrCF2CF2Br, Journal of Fluorine Chemistry 2006, 127, 1195-1203.
21. Jun Li, Yongbin Han, Teresa B. Freedman, Shifa Zhu, Deborah J. Kerwood and Yan-Yeung Luk*, Utilizing the high dielectric constant of water: efficient synthesis of amino acid-derivatized cyclobutenones. Tetrahedron Lett. 2008, 49, 2128-2131.
22. Wan Pang; Shifa Zhu; Huanfeng Jiang; Shizheng Zhu*. A novel synthesis of 5-perfluorophenyl 4,5-dihydro-1H-pyrazoles in THF or water. Journal of Fluorine Chemistry 2007, 128, 1379-1384.
23. Wan Pang; Shifa Zhu; Huanfeng Jiang; Shizheng Zhu*. Rh(II)-catalyzed formation and rearrangement of trifluoroacetyl-containing sulfur ylides. Tetrahedron 2007, 63, 4543-4547.
24. Wan Pang; Shifa Zhu; Chunhui Xing; Nianhua Luo; Huanfeng Jiang; Shizheng Zhu*. Synthesis of stable arsonium and sulfur ylides fromperfluoroalkanesulfonyl diazocarbonyl compoundsand their X-ray diffraction analysis; Journal of Fluorine Chemistry 2008, 129, 343-348.
25. Weibing Liu, Huanfeng Jiang*, Shifa Zhu, et al., Hydroalkylation leading to heterocyclic compounds (Part 2): practical synthesis of polysubstituted 1,2,3,4-tetrahydropyridines through multicomponent reactions (MCRs) . Tetrahedron, 2009, 65(38), 7985.
26. Weibing Liu, Huanfeng Jiang*, Peng Zhou, Shifa Zhu DABCO-Induced [2+2+2] Cycloaddition Reaction of Ethyl Propiolate and Arylaldehydes to Synthesize 4-Aryl-4H-pyrans, Synlett 2009, 20, 3295.
27. Hua Cao, Huanfeng Jiang*, Ronghuan Mai, Shifa Zhu, Chaorong Qi, Silver-Catalyzed One-Pot Cyclization Reaction of Electron- Deficient Alkynes and 2-Yn-1-ols: An Efficient Domino Process to Polysubstituted Furans Adv. Synth. Catal. 2010, 352, 143.
28. Wan Pang, Shifa Zhu, Yong Xin, Huanfeng Jiang, Shizheng Zhu，Rh2(OAc)4 catalyzed formation of fluorine-containing polysubstituted furans from diazocompounds and aromatic alkynes, Tetrahedron, 2010, 66, 1261-1266.
29. Zhengwang Chen, Jinghao Li, Huanfeng Jiang, Shifa Zhu, Yibiao Li and Chaorong Qi, Silver-Catalyzed Difunctionalization of Terminal Alkynes: Highly Regio- and Stereoselective Synthesis of (Z)-β-Haloenol Acetates, Org. Lett. 2010, 12, 3262-3265.
书刊章节:
30. Shifa Zhu, X. Peter Zhang*, “Cobalt (II) Acetate”, in e-EROS Encyclopedia of Reagents for Organic Synthesis; Wiley-Interscience, 2009.
专利:
31. 轴手性咪唑盐化合物及其制备方法，祝诗发，王朝，专利申请号：CN201110008913.4
32. 轴手性邻二胺化合物及其制备方法，祝诗发，王朝，专利申请号：CN201110008898.3
33. 氮杂卡宾金络合物的制备方法，祝诗发，梁仁校，陈丽娟, CN201110107960.4
34. 氮杂卡宾铜络合物的制备方法，祝诗发，梁仁校，陈丽娟, CN201110107949.8
35. 氮杂卡宾银络合物的制备方法，祝诗发，梁仁校，陈丽娟, CN201110107958.7
36. 1-芳基-2-氟代芳基乙烯及其衍生物、其合成和应用。朱仕正、祝诗发，03129584
37. 含氟芳基亚胺化合物及其共晶化合物的合成和应用。朱仕正、祝诗发，00410089085.1
38. Cobalt-catalyzed asymmetric cyclopropanation with diazosulfones. X. Zhang, Shifa Zhu，PCT Int. Appl. (2009), WO 2009114849 A120090917 (美国专利，2009)
39. Peter X. Zhang, Shifa Zhu, Cobalt-Catalyzed Asymmetric Cyclopropanation of Alkene with -nitro-diazoacetates, U.S. Pat. Appl. Publ. (2010), US 2010081838 A120100401 (美国专利, 2010)
招生计划：
硕士生：有机化学 名额： 2-3人
本科生：名额：2-3
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